New Imidazabole Derivatives: Dimers of Carbene–Borane Adducts
Identifieur interne : 001A95 ( Main/Exploration ); précédent : 001A94; suivant : 001A96New Imidazabole Derivatives: Dimers of Carbene–Borane Adducts
Auteurs : Itzia I. Padilla-Martínez [Mexique] ; Francisco J. Martínez-Martínez ; Armando L Pez-Sandoval ; Katia I. Gir N-Castillo ; Marco A. Brito ; Rosalinda Contreras [Mexique]Source :
- European Journal of Inorganic Chemistry [ 1434-1948 ] ; 1998-10.
English descriptors
- Teeft :
- Adduct, Bond length, Bond lengths, Chem, Derivative, Diethyl ether, Dimer, Full paper, Imidazabole, Imidazabole derivatives, Imidazaboles, Imidazole, Imidazole ring, Inorg, Molecular structure, Molecular structures, Niedenzu, Other hand, Pyrazabole analogues, Structure analysis, Trofimenko, Typical range.
Abstract
The preparation and characterization of five new imidazabole derivatives is reported: 1,5‐dibenzyl‐4,4,8,8‐tetrahydroimidazabole (2), 4,4,8,8‐tetrafluoro‐1,5‐dimethylimidazabole (3), 4,4‐difluoro‐8,8‐dihydro‐1,5‐dimethylimidazabole (4), 4,4,8,8‐tetrachloro‐1,5‐dimethylimidazabole (5), and 4,4,8,8‐tetraethyl‐1,5‐dimethylimidazabole (6). The structures of compounds 2–6 as dimeric carbene–borane adducts rather than dimeric N‐borane adducts are discussed on the basis of NMR (2–6) and X‐ray diffraction data (2, 3, 5 and 6).
Url:
DOI: 10.1002/(SICI)1099-0682(199810)1998:10<1547::AID-EJIC1547>3.0.CO;2-5
Affiliations:
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Padilla-Martínez</name><affiliation wicri:level="1"><country wicri:rule="url">Mexique</country></affiliation></author><author><name sortKey="Martinez Artinez, Francisco J" sort="Martinez Artinez, Francisco J" uniqKey="Martinez Artinez F" first="Francisco J." last="Martínez-Martínez">Francisco J. Martínez-Martínez</name><affiliation><wicri:noCountry code="subField">56325</wicri:noCountry></affiliation></author><author><name sortKey="L Pez Andoval, Armando" sort="L Pez Andoval, Armando" uniqKey="L Pez Andoval A" first="Armando" last="L Pez-Sandoval">Armando L Pez-Sandoval</name><affiliation><wicri:noCountry code="subField">56325</wicri:noCountry></affiliation></author><author><name sortKey="Gir N Astillo, Katia I" sort="Gir N Astillo, Katia I" uniqKey="Gir N Astillo K" first="Katia I." last="Gir N-Castillo">Katia I. Gir N-Castillo</name><affiliation><wicri:noCountry code="subField">56325</wicri:noCountry></affiliation></author><author><name sortKey="Brito, Marco A" sort="Brito, Marco A" uniqKey="Brito M" first="Marco A." last="Brito">Marco A. Brito</name><affiliation><wicri:noCountry code="subField">56325</wicri:noCountry></affiliation></author><author><name sortKey="Contreras, Rosalinda" sort="Contreras, Rosalinda" uniqKey="Contreras R" first="Rosalinda" last="Contreras">Rosalinda Contreras</name><affiliation wicri:level="1"><country wicri:rule="url">Mexique</country></affiliation></author></analytic><monogr></monogr><series><title level="j" type="main">European Journal of Inorganic Chemistry</title><title level="j" type="alt">EUROPEAN JOURNAL OF INORGANIC CHEMISTRY</title><idno type="ISSN">1434-1948</idno><idno type="eISSN">1099-0682</idno><imprint><biblScope unit="vol">1998</biblScope><biblScope unit="issue">10</biblScope><biblScope unit="page" from="1547">1547</biblScope><biblScope unit="page" to="1553">1553</biblScope><biblScope unit="page-count">7</biblScope><publisher>WILEY‐VCH Verlag GmbH</publisher><pubPlace>Weinheim</pubPlace><date type="published" when="1998-10">1998-10</date></imprint><idno type="ISSN">1434-1948</idno></series></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">1434-1948</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="Teeft" xml:lang="en"><term>Adduct</term><term>Bond length</term><term>Bond lengths</term><term>Chem</term><term>Derivative</term><term>Diethyl ether</term><term>Dimer</term><term>Full paper</term><term>Imidazabole</term><term>Imidazabole derivatives</term><term>Imidazaboles</term><term>Imidazole</term><term>Imidazole ring</term><term>Inorg</term><term>Molecular structure</term><term>Molecular structures</term><term>Niedenzu</term><term>Other hand</term><term>Pyrazabole analogues</term><term>Structure analysis</term><term>Trofimenko</term><term>Typical range</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The preparation and characterization of five new imidazabole derivatives is reported: 1,5‐dibenzyl‐4,4,8,8‐tetrahydroimidazabole (2), 4,4,8,8‐tetrafluoro‐1,5‐dimethylimidazabole (3), 4,4‐difluoro‐8,8‐dihydro‐1,5‐dimethylimidazabole (4), 4,4,8,8‐tetrachloro‐1,5‐dimethylimidazabole (5), and 4,4,8,8‐tetraethyl‐1,5‐dimethylimidazabole (6). The structures of compounds 2–6 as dimeric carbene–borane adducts rather than dimeric N‐borane adducts are discussed on the basis of NMR (2–6) and X‐ray diffraction data (2, 3, 5 and 6).</div></front></TEI><affiliations><list><country><li>Mexique</li></country></list><tree><noCountry><name sortKey="Brito, Marco A" sort="Brito, Marco A" uniqKey="Brito M" first="Marco A." last="Brito">Marco A. Brito</name><name sortKey="Gir N Astillo, Katia I" sort="Gir N Astillo, Katia I" uniqKey="Gir N Astillo K" first="Katia I." last="Gir N-Castillo">Katia I. Gir N-Castillo</name><name sortKey="L Pez Andoval, Armando" sort="L Pez Andoval, Armando" uniqKey="L Pez Andoval A" first="Armando" last="L Pez-Sandoval">Armando L Pez-Sandoval</name><name sortKey="Martinez Artinez, Francisco J" sort="Martinez Artinez, Francisco J" uniqKey="Martinez Artinez F" first="Francisco J." last="Martínez-Martínez">Francisco J. Martínez-Martínez</name></noCountry><country name="Mexique"><noRegion><name sortKey="Padilla Artinez, Itzia I" sort="Padilla Artinez, Itzia I" uniqKey="Padilla Artinez I" first="Itzia I." last="Padilla-Martínez">Itzia I. Padilla-Martínez</name></noRegion><name sortKey="Contreras, Rosalinda" sort="Contreras, Rosalinda" uniqKey="Contreras R" first="Rosalinda" last="Contreras">Rosalinda Contreras</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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